Weight, Balance & Volume Calibration Protocols Step-by-Step Calibration Protocols for Weights, Balances, and Volumetric Instruments in Pharma Introduction Weight, balance, and volume measurements are foundational to pharmaceutical accuracy. Whether it’s dispensing an API or measuring a reagent for QC testing, ensuring that balances and volumetric devices are properly calibrated is non-negotiable under GMP, GLP, and data integrity requirements. This article provides a comprehensive guide to calibrating analytical balances, reference weights, pipettes, burettes, and volumetric flasks. It aligns with FDA, EMA, and ICH guidelines and uses practical examples and dummy data to support implementation. Applicable Regulations and Standards 21 CFR Part…